6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

Base Information

Chemical Name:6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester
CAS No.:178271-56-2
Molecular Formula:C₄₉H₅₉NO₁₂
Molecular Weight:854.007
Hs Code.:

6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

Synonyms:6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

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Chemical Property of 6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

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Technology Process of 6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

There total 1 articles about 6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 153659-02-0
Dibenzyl 6-deoxy-2,3,4-tri-O-benzyl-β-L-galactopyranosyl phosphite

: 6-((2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-hexanoic acid methyl ester

: 178271-56-2
6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

Guidance literature:: With 4 A molecular sieve; silver perchlorate; zinc(II) chloride; In dichloromethane; at -15 ℃; for 1h;
DOI:10.1021/ja952265x

Reference yield:

: 178271-56-2
6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

: C₆₈H₈₃NO₂₀

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) borane-triethylamine complex, 4A molecular sieves, 2.) AlCl₃ / 1.) THF, RT, 30 min, 2.) THF, RT, 18 h

2: 29 percent / 4A molecular sieves, TMSOTf / CH₂Cl₂ / 20 h / 40 °C

With aluminium trichloride; trimethylsilyl trifluoromethanesulfonate; triethylamine-borane; 4 A molecular sieve; In dichloromethane;
DOI:10.1021/ja952265x

Reference yield:

: 178271-56-2
6-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-hexanoic acid methyl ester

: 178271-52-8
6-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoic acid methyl ester

Guidance literature:: With aluminium trichloride; triethylamine-borane; 4 A molecular sieve; Yield given. Multistep reaction; 1.) THF, RT, 30 min, 2.) THF, RT, 18 h;
DOI:10.1021/ja952265x