methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate

Base Information

Chemical Name:methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate
CAS No.:1067891-53-5
Molecular Formula:C₂₀H₂₁NO₅
Molecular Weight:355.39
Hs Code.:

Synonyms:methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate

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Chemical Property of methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate

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Technology Process of methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate

There total 3 articles about methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₁NO₄

: 1067891-53-5
methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1021/ol801860s

Reference yield:

: 875118-61-9
methyl 4-(((benzyloxy)carbonyl)amino)benzoate

: 1067891-53-5
methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C

1.2: 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 1067891-53-5
methyl 4-((benzyloxycarbonyl)((2-methyloxiran-2-yl)methyl)amino)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran / 0 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C

2.2: 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C

With sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;