N,N-diallyl-5-chloro-2-methoxyaniline

Base Information

• Chemical Name: N,N-diallyl-5-chloro-2-methoxyaniline
• CAS No.: 1384245-86-6
• Molecular Formula: C₁₃H₁₆ClNO
• Molecular Weight: 237.729
• Mol file: 1384245-86-6.mol

Synonyms:N,N-diallyl-5-chloro-2-methoxyaniline

Chemical Property of N,N-diallyl-5-chloro-2-methoxyaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N,N-diallyl-5-chloro-2-methoxyaniline

There total 1 articles about N,N-diallyl-5-chloro-2-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

allyl bromide (106-95-6) + 5-chloro-2-methoxyaniline (95-03-4) → N,N-diallyl-5-chloro-2-methoxyaniline (1384245-86-6)

Guidance literature:

With sodium carbonate; In ethanol; water; at 80 ℃; Inert atmosphere;

DOI:10.1039/c2ob25543j

Reference yield:

N,N-diallyl-5-chloro-2-methoxyaniline (1384245-86-6) → C11H12ClNO

Guidance literature:

With Grubbs catalyst first generation; In benzene; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1039/c2ob25543j

Reference yield:

N,N-diallyl-5-chloro-2-methoxyaniline (1384245-86-6) → 1-(5-chloro-2-methoxyphenyl)-1H-pyrrole (158966-65-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Grubbs catalyst first generation / benzene / 0.5 h / 20 °C / Inert atmosphere

2: tert.-butylhydroperoxide / water; benzene / 0.5 h / 20 °C / Inert atmosphere

With Grubbs catalyst first generation; tert.-butylhydroperoxide; In water; benzene;

DOI:10.1039/c2ob25543j

upstream raw materials:

allyl bromide

5-chloro-2-methoxyaniline

Downstream raw materials:

1-(5-chloro-2-methoxyphenyl)-1H-pyrrole