2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate

Base Information

Chemical Name:2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate
CAS No.:855297-15-3
Molecular Formula:C₂₄H₄₂N₂O₃Si
Molecular Weight:434.695
Hs Code.:

Synonyms:2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate

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Chemical Property of 2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate

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Technology Process of 2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate

There total 3 articles about 2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 855297-19-7
2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)carbamate

: 855297-15-3
2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate

Guidance literature:: With acetic anhydride; acetic acid; sodium nitrite; at 5 - 20 ℃; for 14h;
DOI:10.1016/j.tet.2005.03.044

Reference yield:

: 18135-04-1
2-(trimethylsilyl)ethan-1-amine

: 855297-15-3
2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / pyridine / CH₂Cl₂ / 12 h / 0 - 20 °C

2: 84 percent / acetic acid; acetic anhydride; sodium nitrite / 14 h / 5 - 20 °C

With pyridine; acetic anhydride; acetic acid; sodium nitrite; In dichloromethane;
DOI:10.1016/j.tet.2005.03.044

Reference yield:

: 4511-21-1
2,4,6-tri(tert-butyl)phenyl carbonochloridate

: 855297-15-3
2,4,6-tris(t-butyl)phenyl N-(2-trimethylsilylethyl)-N-nitrosocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / pyridine / CH₂Cl₂ / 12 h / 0 - 20 °C

2: 84 percent / acetic acid; acetic anhydride; sodium nitrite / 14 h / 5 - 20 °C

With pyridine; acetic anhydride; acetic acid; sodium nitrite; In dichloromethane;
DOI:10.1016/j.tet.2005.03.044