N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide

Base Information

Chemical Name:N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide
CAS No.:588717-92-4
Molecular Formula:C₂₉H₃₅N₃O₉
Molecular Weight:569.612
Hs Code.:

Synonyms:N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide

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Chemical Property of N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide

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Technology Process of N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide

There total 2 articles about N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 2420-94-2
2-aminoethylmethacrylate hydrochloride

: Succinic acid mono-[(2S,4S)-4-hydroxycarbamoyl-2-(4-phenoxy-benzoylamino)-pentyl] ester

: 588717-92-4
N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at -5 - 20 ℃;
DOI:10.1021/jm020356g

Reference yield:

: 223471-02-1
ONO-M₁₁-335

: 588717-92-4
N-hydroxy-5-[2-[N-[2-(isopropenylcarbonyloxy)ethyl]carbamoyl]ethylcarbonyloxy]-2(S)-methyl-4(S)-(4-phenoxybenzoyl)aminopentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / pyridine / 20 °C

2: 55 percent / HOBt; NEt₃; DCC / dimethylformamide / -5 - 20 °C

With pyridine; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jm020356g