[(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride

Base Information

Chemical Name:[(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride
CAS No.:1421592-02-0
Molecular Formula:C₄₂H₆₁ClO₅PV
Molecular Weight:763.312
Hs Code.:

Synonyms:[(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride

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Chemical Property of [(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride

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Technology Process of [(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride

There total 2 articles about [(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 131063-11-1,16997-51-6,19559-06-9
Vanadium (III) chloride-(tris-tetrahydrofuran)

: 140687-31-6
bis(3,5-di-tert-butyl-2-hydroxyphenyl)phenylphosphine(V) oxide

: 1421592-02-0
[(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/pola.26441

Reference yield:

: bis(3,5-di-tert-butyl-2-hydroxyphenyl)phenylphosphine

: 1421592-02-0
[(ditetrahydrofuran)(bis(3,5-di-tert-butyl-2-phenoxy)phenylphosphine oxide)]vanadium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / Inert atmosphere; Schlenk technique

2: triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

With dihydrogen peroxide; triethylamine; In tetrahydrofuran;
DOI:10.1002/pola.26441