C₂₆H₂₂N₂O₂

Base Information

Chemical Name:C₂₆H₂₂N₂O₂
CAS No.:1360445-18-6
Molecular Formula:C₂₆H₂₂N₂O₂
Molecular Weight:394.473
Hs Code.:

C<sub>26</sub>H<sub>22</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₆H₂₂N₂O₂

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Chemical Property of C₂₆H₂₂N₂O₂

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Technology Process of C₂₆H₂₂N₂O₂

There total 5 articles about C₂₆H₂₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78725-70-9
C₁₀H₉BrO₂

: 1360445-18-6
C₂₆H₂₂N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: Jones reagent / acetone / 0.5 h / 0 °C / Inert atmosphere

2.1: sodium carbonate / acetonitrile / 8 h / Reflux; Inert atmosphere

3.1: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.67 h / 20 °C / Inert atmosphere

4.2: 16 h / Inert atmosphere; Reflux

With Jones reagent; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron dimethyl-trifluoro sulphide; sodium carbonate; In 1,2-dimethoxyethane; dichloromethane; 1,2-dichloro-ethane; acetone; acetonitrile; 4.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015

Reference yield:

: 78725-40-3
C₁₀H₇BrO₂

: 1360445-18-6
C₂₆H₂₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / acetonitrile / 8 h / Reflux; Inert atmosphere

2.1: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.67 h / 20 °C / Inert atmosphere

3.2: 16 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron dimethyl-trifluoro sulphide; sodium carbonate; In 1,2-dimethoxyethane; dichloromethane; 1,2-dichloro-ethane; acetonitrile; 3.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015

Reference yield:

: 1360444-95-6
C₁₇H₁₃BrN₂O

: 1360445-18-6
C₂₆H₂₂N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.67 h / 20 °C / Inert atmosphere

2.2: 16 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron dimethyl-trifluoro sulphide; In 1,2-dimethoxyethane; dichloromethane; 1,2-dichloro-ethane; 2.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015