diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate

Base Information

Chemical Name:diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate
CAS No.:58370-38-0
Molecular Formula:C₂₄H₃₂N₂O₇P₂
Molecular Weight:522.475
Hs Code.:

Synonyms:diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate

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Chemical Property of diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate

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Technology Process of diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate

There total 9 articles about diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 58370-39-1
2,5-bis[4-(bromomethyl)phenyl]-1,3,4-oxadia-zole

: 122-52-1
triethyl phosphite

: 58370-38-0
diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate

Guidance literature:: at 150 ℃; for 3h;
DOI:10.1021/ma035576y

Reference yield:

: 2491-91-0
2,5-di-p-tolyl-1,3,4-oxadiazole

: 58370-38-0
diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / N-bromosuccinimide; benzoyl peroxide / benzene / 3 h / 85 °C

2: 98 percent / 3 h / 150 °C

With N-Bromosuccinimide; dibenzoyl peroxide; In benzene;
DOI:10.1021/ma035576y

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 58370-38-0
diethyl 4-(5-(4-(diethoxyphosphino)methylphenyl)-1,3,4-oxadiazol-2-yl)-benzyl-phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / NH₂NH₂*2HCl; polyphosphoric acid / 6 h / 150 - 200 °C

2: 34 percent / N-bromosuccinimide; benzoyl peroxide / benzene / 3 h / 85 °C

3: 98 percent / 3 h / 150 °C

With N-Bromosuccinimide; PPA; hydrazine dihydrochloride; dibenzoyl peroxide; In benzene;
DOI:10.1021/ma035576y