((C₆H₅CH₂)2C₂B₄H₄)2FeH₂

Base Information

Chemical Name:((C₆H₅CH₂)2C₂B₄H₄)2FeH₂
CAS No.:105472-94-4
Molecular Formula:C₃₂H₃₈B₈Fe
Molecular Weight:564.989
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>)2C<sub>2</sub>B<sub>4</sub>H<sub>4</sub>)2FeH<sub>2</sub>

Synonyms:((C₆H₅CH₂)2C₂B₄H₄)2FeH₂

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Chemical Property of ((C₆H₅CH₂)2C₂B₄H₄)2FeH₂

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Technology Process of ((C₆H₅CH₂)2C₂B₄H₄)2FeH₂

There total 1 articles about ((C₆H₅CH₂)2C₂B₄H₄)2FeH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: (C₆H₅CH₂)2C₂B₄H₅^(1-)

: iron(II) chloride

: 105472-94-4
((C₆H₅CH₂)2C₂B₄H₄)2FeH₂

Guidance literature:: In tetrahydrofuran; Mixt. of reagents in THF was stirred on a dry ice-acetone bath for 2 h, then slowly warmed to room temp. followed by stirring for 15 min;; Solvent was quickly removed in vac.; residue was dissolved in benzene ( N2 atm.), filtered, solid was washed with benzene, residue was sublimed at 70°C and 10E-5 torr;;

Reference yield: 48.0%

: 105472-94-4
((C₆H₅CH₂)2C₂B₄H₄)2FeH₂

: 105472-95-5
(C₆H₅CH₂)4C₄B₈H₈

Guidance literature:: With O₂; In dichloromethane; O2 gas was bubbled through the soln. of complex in CH2Cl2 for 30 min, then exposure to air for 12 h;; soln. was filtered, solvent removed, recrystd. from CH2Cl2;;

Reference yield: 28.0%

: 12078-25-0,12078-23-8
dicarbonylcyclopentadienylcobalt

: 105472-94-4
((C₆H₅CH₂)2C₂B₄H₄)2FeH₂

: 105501-04-0
{(PhCH2)2C2B4H4}2FeCo(η5-C5H5)

Guidance literature:: In benzene; Irradiation (UV/VIS); Soln. of reagents in benzene was irradiated under N2 atm. for 5 h with constant stirring;; reactor was opened to the atm., soln. was filtered through silica gel, washed with CH2Cl2, evapd.; chromd. on silica gel TLC plates, eluent CH2Cl2 hexane;;