10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione

Base Information

Chemical Name:10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione
CAS No.:1338685-12-3
Molecular Formula:C₂₆H₂₉ClN₄O₃
Molecular Weight:480.994
Hs Code.:

Synonyms:10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione

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Chemical Property of 10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione

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Technology Process of 10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione

There total 10 articles about 10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63649-64-9
4-isopropyl-2-nitrobenzenamine

: 1338685-12-3
10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

1.2: 18 h / 20 °C

2.1: hydrogen / ethanol / 2 h / 760.05 Torr

3.1: boric acid; acetic acid / 18 h / 20 °C

With hydrogen; boric acid; sodium hydride; acetic acid; In ethanol; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 61066-33-9,61066-34-0,61066-35-1,61127-23-9
pyrimidine-2,4,5,6(1H,3H)-tetraone

: 1338685-19-0
N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

: 1338685-12-3
10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: With boric acid; acetic acid; at 20 ℃; for 18h;

Reference yield:

: 1338685-13-4
isobutyl 3-(4-chlorophenyl)-2-isobutoxyacrylate

: 1338685-12-3
10-[3-(4-chlorophenyl)-2-isobutoxypropyl]-7-isopropylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen; zinc dibromide / palladium 10% on activated carbon / ethyl acetate / 42 h / 20 °C / 760.05 Torr

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C

3.1: triphenylphosphine; bromine / dichloromethane / 24.5 h / 0 - 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

4.2: 18 h / 20 °C

5.1: hydrogen / ethanol / 2 h / 760.05 Torr

6.1: boric acid; acetic acid / 18 h / 20 °C

With lithium aluminium tetrahydride; hydrogen; bromine; boric acid; sodium hydride; acetic acid; triphenylphosphine; zinc dibromide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;