2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester

Base Information

Chemical Name:2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester
CAS No.:326596-83-2
Molecular Formula:C₃₅H₄₁NO₄S
Molecular Weight:571.781
Hs Code.:

Synonyms:2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester

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Chemical Property of 2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester

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Technology Process of 2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester

There total 1 articles about 2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5-(9H-fluoren-9-ylmethoxycarbonylamino)-3-hydroxy-2-isobutyl-6-phenyl-4-phenylselanylhexanethioic acid S-tert-butyl ester

: 326596-83-2
2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester

Guidance literature:: With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; at -15 ℃; for 0.5h;
DOI:10.1021/jo000961w

Reference yield:

: 326596-83-2
2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester

: (S)-2-{(2R,3R)-3-[(S)-1-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-phenyl-ethyl]-oxiranyl}-4-methyl-pentanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo000961w

Reference yield:

: 326596-83-2
2-{3-[1-(9H-fluoren-9-ylmethoxycarbonylamino)-2-phenylethyl]oxiranyl}-4-methylpentanethioic acid S-tert-butyl ester

: (S)-2-{(2R,3R)-3-[(S)-1-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-phenyl-ethyl]-oxiranyl}-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.2 M NaOH / tetrahydrofuran / 20 °C

2: diethyl ether; tetrahydrofuran / -15 °C

With sodium hydroxide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo000961w