C₄₅H₈₄O₉

Base Information

Chemical Name:C₄₅H₈₄O₉
CAS No.:1424713-00-7
Molecular Formula:C₄₅H₈₄O₉
Molecular Weight:769.157
Hs Code.:

C<sub>45</sub>H<sub>84</sub>O<sub>9</sub>

Synonyms:C₄₅H₈₄O₉

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Chemical Property of C₄₅H₈₄O₉

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Technology Process of C₄₅H₈₄O₉

There total 18 articles about C₄₅H₈₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1433995-47-1
C₅₇H₁₀₀O₉

: 1424713-00-7
C₄₅H₈₄O₉

Guidance literature:: With acetic acid; In methanol; at 20 ℃; for 48h;
DOI:10.1055/s-0032-1317929

Reference yield:

: C₂₂H₄₀O₅

: 1424713-00-7
C₄₅H₈₄O₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrahydrofuran / 12 h / 65 °C

2.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / -10 °C / Inert atmosphere

4.1: sodium; methanol / 1 h / 0 - 20 °C / Inert atmosphere

5.1: pyridine / 72 h / 110 °C

6.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

8.2: 0 - 20 °C / Inert atmosphere

9.1: acetic acid / methanol / 48 h / 20 °C

With pyridine; methanol; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; sodium; sodium hydride; diisobutylaluminium hydride; potassium carbonate; acetic acid; triphenylphosphine; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: |Mitsunobu Displacement / 8.2: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929

Reference yield:

: 1424712-86-6
C₅₁H₉₀O₁₀

: 1424713-00-7
C₄₅H₈₄O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: acetic acid / methanol / 48 h / 20 °C

With lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; mineral oil; 3.2: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929