7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one

Base Information

• Chemical Name: 7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one
• CAS No.: 1329019-50-2
• Molecular Formula: C₁₈H₁₃ClN₄O₂S
• Molecular Weight: 384.846

Synonyms:7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one

Chemical Property of 7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one

Chemical Property:

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Technology Process of 7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one

There total 3 articles about 7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-amino-3-(2-p-chlorophenyl-2-oxo-ethylsulfanyl)-6-p-methoxyphenyl-4H-[1,2,4]triazin-5-one (1179505-05-5) → 7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one (1329019-50-2)

Guidance literature:

With toluene-4-sulfonic acid; In ethanol; Reflux;

DOI:10.1016/j.tet.2011.06.034

Reference yield:

C10H10N4O2S (619297-80-2) → 7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one (1329019-50-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 2 h / 20 °C

2: toluene-4-sulfonic acid / ethanol / Reflux

With potassium carbonate; toluene-4-sulfonic acid; In ethanol; acetonitrile;

DOI:10.1016/j.tet.2011.06.034

Reference yield:

4-chlorobenzoylmethyl bromide (536-38-9) → 7-p-chlorophenyl-3-p-methoxyphenyl-8H-[1,2,4]triazino[3,4-b][1,3,4] thiadiazin-4-one (1329019-50-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 2 h / 20 °C

2: toluene-4-sulfonic acid / ethanol / Reflux

With potassium carbonate; toluene-4-sulfonic acid; In ethanol; acetonitrile;

DOI:10.1016/j.tet.2011.06.034

upstream raw materials:

C₁₀H₁₀N₄O₂S

4-amino-3-(2-p-chlorophenyl-2-oxo-ethylsulfanyl)-6-p-methoxyphenyl-4H-[1,2,4]triazin-5-one

4-chlorobenzoylmethyl bromide

Downstream raw materials:

7-p-chlorophenyl-3-p-methoxyphenyl-1H-pyrazolo[5,1-c][1,2,4]triazin-4-one

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