(Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Base Information

Chemical Name:(Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone
CAS No.:77879-12-0
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:

Synonyms:(Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Chemical Property:

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Technology Process of (Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

There total 4 articles about (Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3066-90-8
2,3-dimethoxy-5-methylbenzene-1,4-diol

: 77878-75-2
(Z),(E)-3-methyl-2-hexene-1,6-diol

: 77879-12-0
(Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: With diethyl ether; boron trifluoride; iron(III) chloride; Yield given. Multistep reaction; 1.) dioxane, RT, 90 min, 2.) dioxane/aq. MeOH, RT, 30 min;
DOI:10.1248/cpb.30.2797

Reference yield:

: 624-45-3
levulinic acid methyl ester

: 77879-12-0
(Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / xylene / 24 h / Heating

2: 86 percent / LiAlH₄ / diethyl ether / 1.17 h / -20 °C

3: 1.) BF₃/Et₂O, 2.) FeCl₃ / 1.) dioxane, RT, 90 min, 2.) dioxane/aq. MeOH, RT, 30 min

With lithium aluminium tetrahydride; diethyl ether; boron trifluoride; iron(III) chloride; In diethyl ether; xylene;
DOI:10.1248/cpb.30.2797

Reference yield:

: 77878-74-1
(Z),(E)-ethyl 5-methoxycarbonyl-3-methyl-2-pentenoate

: 77879-12-0
(Z),(E)-6-(hydroxy-3-methyl-2-hexenyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / LiAlH₄ / diethyl ether / 1.17 h / -20 °C

2: 1.) BF₃/Et₂O, 2.) FeCl₃ / 1.) dioxane, RT, 90 min, 2.) dioxane/aq. MeOH, RT, 30 min

With lithium aluminium tetrahydride; diethyl ether; boron trifluoride; iron(III) chloride; In diethyl ether;
DOI:10.1248/cpb.30.2797