8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin

Base Information

Chemical Name:8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin
CAS No.:42607-17-0
Molecular Formula:C₃₈H₄₂N₄O₆
Molecular Weight:650.775
Hs Code.:

Synonyms:8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin

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Chemical Property of 8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin

There total 4 articles about 8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2624-63-7
coproporphyrinogen III

: 42607-17-0
8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin

: 5522-66-7,6164-53-0
3,3'-(3,7,12,17-tetramethyl-8,13-divinyl-21H,23H-porphine-2,18-diyl)-bis-propionic acid dimethyl ester

: 5522-63-4
coproporphyrin III tetramethyl ester

Guidance literature:: for 0.5h; coproporphyrinogen-III oxidase (from Euglena gracilis);

Reference yield:

: 4792-10-3
3-{5-Formyl-2-[5-formyl-3-(2-methoxycarbonyl-ethyl)-4-methyl-1H-pyrrol-2-ylmethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid methyl ester

: 42607-17-0
8,13,17-tris(2-methoxycarbonylethyl)-2,7,12,18-tetramethyl-3-vinylporphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / 1.) trifluoroacetic acid, 2.) sodium acetate / methanol; CH₂Cl₂ / 1.) 2-3 deg C 90 min, 2.) 18 deg C 5 min, 3.) 50 min

2: 1.) 2M aq. potassium hydroxide; 2.) sodium amalgam / 1.) tetrahydrofuran 20 deg C; 2.) 3-4 min

3: 0.5 h / coproporphyrinogen-III oxidase (from Euglena gracilis)

With potassium hydroxide; sodium amalgam; sodium acetate; trifluoroacetic acid; In methanol; dichloromethane;