(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide

Base Information

Chemical Name:(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide
CAS No.:338731-17-2
Molecular Formula:C₂₁H₂₆N₂O₆
Molecular Weight:402.447
Hs Code.:

Synonyms:(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide

Suppliers and Price of (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide

There total 2 articles about (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 4393-09-3
2,3-dimethoxybenzyl amine

: 338731-15-0
N-2,3-Dimethoxybenzoyl-L-alanine

: 338731-17-2
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide

Guidance literature:: N-2,3-Dimethoxybenzoyl-L-alanine; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In 1,4-dioxane; at 20 ℃; for 16h;

2,3-dimethoxybenzyl amine; With sodium hydrogencarbonate; In water; for 20h;
DOI:10.1055/s-2001-11438

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 338731-17-2
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl) ethyl amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: DCC; N-hydroxysuccinimide / dioxane / 17 h / 20 °C

1.2: 87 percent / NaHCO₃ / H₂O / 19 h

2.1: DCC; N-hydroxysuccinimide / dioxane / 16 h / 20 °C

2.2: 73 percent / NaHCO₃ / H₂O / 20 h

With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1055/s-2001-11438