C₂₁H₃₃N₃

Base Information

Chemical Name:C₂₁H₃₃N₃
CAS No.:174753-36-7
Molecular Formula:C₂₁H₃₃N₃
Molecular Weight:327.513
Hs Code.:

C<sub>21</sub>H<sub>33</sub>N<sub>3</sub>

Synonyms:C₂₁H₃₃N₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₃N₃

Chemical Property:

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Technology Process of C₂₁H₃₃N₃

There total 15 articles about C₂₁H₃₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 174753-18-5
1-(diethyltriazenyl)-3-(3'-ethylheptyl)-4-<(trimethylsilyl)ethynyl>benzene

: 174753-36-7
C₂₁H₃₃N₃

Guidance literature:: With methanol; potassium carbonate; at 23 ℃;

Reference yield:

: 187871-22-3
4-amino-2-(3'-ethylheptyl)acetophenone

: 174753-36-7
C₂₁H₃₃N₃

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) t-BuONO, BF₃-OEt₂, 2.) K₂CO₃ / 1.) CH₂Cl₂, 0 deg C, 30 min, 2.) 1 h

3: 96 percent / TBAF / tetrahydrofuran

With tert.-butylnitrite; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran;
DOI:10.1021/jo962336q

Reference yield:

: 187871-08-5
1-(3'-nitrophenyl)-3-ethylheptane-1-ol

: 174753-36-7
C₂₁H₃₃N₃

Guidance literature:: Multi-step reaction with 8 steps

1: 97 percent / 4-(N,N-dimethylamino)pyridine / pyridine / 0.17 h / 0 °C

2: 60 percent / liq. NH₃, Li / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) -33 deg C, 1 h

3: 87 percent / 1 N NaOH / tetrahydrofuran / 2 h / Heating

4: AlCl₃ / CS₂ / 3 h / 70 °C

5: 3 N NaOH

6: 1.) t-BuONO, BF₃-OEt₂, 2.) K₂CO₃ / 1.) CH₂Cl₂, 0 deg C, 30 min, 2.) 1 h

8: 96 percent / TBAF / tetrahydrofuran

With dmap; sodium hydroxide; aluminium trichloride; tert.-butylnitrite; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; ammonia; lithium; potassium carbonate; In tetrahydrofuran; pyridine; carbon disulfide;
DOI:10.1021/jo962336q