Technology Process of C61H95N3O15S
There total 10 articles about C61H95N3O15S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C42H73NO13S2;
With
tributylphosphine; water;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 2h;
Inert atmosphere;
(2-chloro-ethyl)-(3-cyclopentyloxy-4-methoxy-phenyl)-(pyridin-4-ylmethyl)-amine;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
N,N-dimethyl-formamide;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 5 h / Reflux
1.2: 12 h / 60 °C
2.1: dichloromethane / 4 h / 10 °C / Molecular sieve
3.1: tributylphosphine; water / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
tributylphosphine; water;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
1.2: 0 °C
2.1: sodium cyanoborohydride; acetic acid / methanol; water / 16 h / 25 °C
3.1: tributylphosphine; water / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; tributylphosphine; water; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;