(1R)-1-(3,4-dimethoxyphenyl)ethan-1-ol

Base Information

Chemical Name:(1R)-1-(3,4-dimethoxyphenyl)ethan-1-ol
CAS No.:120466-67-3
Molecular Formula:C₁₀H₁₄O₃
Molecular Weight:182.219
Hs Code.:
European Community (EC) Number:862-428-1
DSSTox Substance ID:DTXSID601266469
Nikkaji Number:J585.022C

Synonyms:(1R)-1-(3,4-dimethoxyphenyl)ethan-1-ol;120466-67-3;(1R)-1-(3,4-DIMETHOXYPHENYL)ETHANOL;SCHEMBL8238025;DTXSID601266469;CS-0250978;EN300-53064;G57115;(alphaR)-3,4-Dimethoxy-alpha-methylbenzenemethanol

Suppliers and Price of (1R)-1-(3,4-dimethoxyphenyl)ethan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (1R)-1-(3,4-dimethoxyphenyl)ethan-1-ol

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:182.094294304
Heavy Atom Count:13
Complexity:149

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C1=CC(=C(C=C1)OC)OC)O
Isomeric SMILES:C[C@H](C1=CC(=C(C=C1)OC)OC)O

Technology Process of (1R)-1-(3,4-dimethoxyphenyl)ethan-1-ol

There total 6 articles about (1R)-1-(3,4-dimethoxyphenyl)ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: 120466-67-3
(R)-methyl(3,4-dimethoxyphenyl)methanol

Guidance literature:: 1-(3,4-dimethoxyphenyl)ethanone; With cobalt(II) acetate; bis-[2-((4S)-4-phenyl-4,5-dihydro-oxazol-2-yl)-phenyl]-amine; In tetrahydrofuran; at 65 ℃; Inert atmosphere;

With diethoxymethylane; In tetrahydrofuran; at 65 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/chem.200903118

Reference yield: 98.0%

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: (S)-1-(3,4-dimethoxyphenyl)ethanol

: 120466-67-3
(R)-methyl(3,4-dimethoxyphenyl)methanol

Guidance literature:: With (mer-[(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene^(1-)]Ru(CO)Cl)2(ZnCl₂); hydrogen; sodium methylate; (-)-(S)-1-Anthracen-9-ylethanol; In isopropyl alcohol; at 40 ℃; for 24h; under 22801.5 Torr; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Autoclave;
DOI:10.1039/c1cc16057e

Reference yield:

: 5653-65-6
1-(3,4-dimethoxyphenyl)ethanol

: (S)-1-(3,4-dimethoxyphenyl)ethanol

: 120466-67-3
(R)-methyl(3,4-dimethoxyphenyl)methanol

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

Guidance literature:: With (1R,2S,9S)-11-methyl-13-oxa-7,11-diazatricyclo[7.3.1.0^2,7]tridecane; C₁₁H₂₀Br₂N₂OPd; oxygen; caesium carbonate; In chloroform; at 20 ℃; for 21.6h; optical yield given as %ee; Molecular sieve;
DOI:10.1021/jo802409x