2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate

Base Information

Chemical Name:2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate
CAS No.:1361382-81-1
Molecular Formula:C₄₁H₃₈F₃NO₅S
Molecular Weight:713.818
Hs Code.:

Synonyms:2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate

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Chemical Property of 2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate

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Technology Process of 2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate

There total 4 articles about 2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361382-80-0
methyl 2,3,4-tri-O-benzyl-6-deox-6-S-phenyl-6-thio-α-D-mannopyranoside

: 1361382-81-1
2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 1.5 h

2: piperidine / tetrahydrofuran / 20 °C

3: caesium carbonate / water; acetone / 72 h

With piperidine; sulfuric acid; caesium carbonate; In tetrahydrofuran; water; acetone;
DOI:10.1039/c2cc17623h

Reference yield:

: C₃₅H₃₆O₆S

: 1361382-81-1
2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / tetrahydrofuran / 20 °C

2: caesium carbonate / water; acetone / 72 h

With piperidine; caesium carbonate; In tetrahydrofuran; water; acetone;
DOI:10.1039/c2cc17623h

Reference yield:

: 108-98-5
thiophenol

: 1361382-81-1
2,3,4-tri-O-benzyl-6-deoxy-6-S-phenyl-6-thio-α-D-mannopyranosyl (N-phenyl)trifluoroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: sulfuric acid / 1.5 h

3: piperidine / tetrahydrofuran / 20 °C

4: caesium carbonate / water; acetone / 72 h

With piperidine; sulfuric acid; caesium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c2cc17623h