diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

Base Information

Chemical Name:diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate
CAS No.:1338382-31-2
Molecular Formula:C₁₇H₂₄NO₆P
Molecular Weight:369.354
Hs Code.:

Synonyms:diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

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Chemical Property of diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

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Technology Process of diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

There total 1 articles about diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 195727-70-9
1-Benzoyl-2-methoxy-5-(methoxycarbonyl)pyrrolidine

: 122-52-1
triethyl phosphite

: 1338382-31-2
diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

: 1346907-17-2
diethyl [N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.080

Reference yield:

: 1338382-31-2
diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

: C₁₆H₂₂NO₆P

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1016/j.tet.2011.09.080

Reference yield:

: 1338382-31-2
diethyl [(5R)-N-benzoyl-(2S)-methoxycarbonylpyrrolidin-5-yl]phosphonate

: diethyl [(2R)-N-benzoyl-5-methoxypyrrolidin-2-yl]phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / tetrahydrofuran; water / 12 h / 20 °C

2: 2,6-dimethylpyridine / 0 °C / Electrochemical reaction

With 2,6-dimethylpyridine; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2011.09.080