Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester

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Chemical Name:Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester
CAS No.:151397-38-5
Molecular Formula:C₂₇H₂₅N₃O₇
Molecular Weight:503.511
Hs Code.:

Synonyms:Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester

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Chemical Property of Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester

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Technology Process of Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester

There total 1 articles about Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2136-75-6
(triphenylphosphoranylidene)acetaldehyde

: 146961-97-9
N⁴-benzoyl-5-methyl-2'-deoxy-3'-O-(phenoxyacetyl)cytidine

: 151397-38-5
Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester

Guidance literature:: With dimethyl sulfoxide; dicyclohexyl-carbodiimide; Multistep reaction;
DOI:10.1021/ja00074a065

Reference yield:

: 151397-38-5
Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester

: Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-(3-oxo-propyl)-tetrahydro-furan-3-yl ester

Guidance literature:: With hydrogen; palladium on activated charcoal;
DOI:10.1021/ja00074a065

Reference yield:

: 151397-38-5
Phenoxy-acetic acid (2R,3S,5R)-5-(4-benzoylamino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-((E)-3-oxo-propenyl)-tetrahydro-furan-3-yl ester

: C₄₈H₄₈N₅O₁₂P*C₆H₁₅N

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / Pd/C

3: CH₃SO₃H

4: NH₃OH

6: C₆H₄-o-, Et₃N

With 2-Chloro-4H-1,3,2-benzodioxaphosphorin-4-one; methanesulfonic acid; hydrogen; triethylamine; palladium on activated charcoal;
DOI:10.1021/ja00074a065