1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene

Base Information

Chemical Name:1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene
CAS No.:1016636-73-9
Molecular Formula:C₂₇H₃₆O₃
Molecular Weight:408.581
Hs Code.:

Synonyms:1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene

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Chemical Property of 1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene

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Technology Process of 1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene

There total 1 articles about 1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1016636-85-3
diethyl (3,5-di-tert-butyl-4-methoxybenzyl)phosphonate

: 121362-78-5
(E)-3-(3,5-dimethoxyphenyl)acrylaldehyde

: 1016636-73-9
1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene

Guidance literature:: diethyl (3,5-di-tert-butyl-4-methoxybenzyl)phosphonate; With potassium tert-butylate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

(E)-3-(3,5-dimethoxyphenyl)acrylaldehyde; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2010.11.018

Reference yield: 77.0%

: 1016636-73-9
1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene

: 1016636-87-5
5-{(1E,3E)-4-[3,5-di-tert-butyl-4-methoxyphenyl]-1,3-butadienyl}-1,3-benzenediol

Guidance literature:: 1,3-di-tert-butyl-5-[(1E,3E)-4-(3,5-dimethoxyphenyl)-1,3-butadienyl]-2-methoxybenzene; With methyl magnesium iodide; In diethyl ether; at 160 ℃; for 2h; Inert atmosphere;

With ammonium chloride; In diethyl ether;
DOI:10.1016/j.bmc.2010.11.018