dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ⁴-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester

Base Information

• Chemical Name: dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ⁴-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester
• CAS No.: 762243-71-0
• Molecular Formula: C₁₈H₂₅NO₃S₄
• Molecular Weight: 431.665

Synonyms:dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ⁴-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester

Chemical Property of dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ⁴-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester

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Technology Process of dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ⁴-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester

There total 2 articles about dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ⁴-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

N-allyl-N-phenylacetamide (55487-54-2) + dithiocarbonic acid O-ethyl ester S-(1-oxo-1λ4-[1,3]dithian-2-yl) ester → dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ4-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester (762243-71-0)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;

DOI:10.1016/j.tet.2004.06.061

Reference yield:

dithiocarbonic acid S-[1,3]dithian-2-yl ester O-ethyl ester (762243-57-2) → dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ4-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester (762243-71-0)

Guidance literature:

Multi-step reaction with 2 steps

1: mCPBA / CH₂Cl₂ / 0 - 20 °C

2: 75 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1,2-dichloro-ethane;

DOI:10.1016/j.tet.2004.06.061

Reference yield: 77.0%

dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-(1-oxo-1λ4-[1,3]dithian-2-ylmethyl)-ethyl] ester O-ethyl ester (762243-71-0) → dithiocarbonic acid S-[2-(acetyl-phenyl-amino)-1-[1,3]dithian-2-ylmethyl-ethyl] ester O-ethyl ester

Guidance literature:

With trifluoroacetic anhydride; sodium iodide; In acetone; at 0 - 20 ℃;

DOI:10.1016/j.tet.2004.06.061

upstream raw materials:

N-allyl-N-phenylacetamide

dithiocarbonic acid S-[1,3]dithian-2-yl ester O-ethyl ester

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