phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside

Base Information

Chemical Name:phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside
CAS No.:1447801-69-5
Molecular Formula:C₄₁H₅₄O₉SSi
Molecular Weight:751.026
Hs Code.:

Synonyms:phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside

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Chemical Property of phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside

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Technology Process of phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside

There total 1 articles about phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-Lidopyranoside

: 217300-17-9
chloromethoxy-triisopropyl-silane

: 1447801-69-5
phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo400467g

Reference yield: 91.0%

: 1276114-12-5
4-((benzyl(5-hydroxypentyl)carbamoyloxy)methyl)benzyl benzoate

: 1447801-69-5
phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside

: 1447801-92-4
4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-6-O-[(triisopropylsiloxy)-methyl]-α-L-idopyranosyl)oxy)pentyl]carbamate

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo400467g

Reference yield:

: 1447801-69-5
phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-6-O-[(triisopropylsiloxy)methyl]-α-L-idopyranoside

: 1447802-06-3
4-(phenylcarboxymethyl)benzyl N-benzyl N-(5-(2-O-benzoyl-3-O-benzyl-6-O-tri-iso-propylsiloxymethyl-α-L-idopyranosyloxy)pentyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 - 20 °C / Inert atmosphere

2: hydrazinium monoacetate / dichloromethane; methanol

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; hydrazinium monoacetate; In methanol; dichloromethane;
DOI:10.1021/jo400467g