α--4-nitrophenylacetonitrile

Base Information

Chemical Name:α--4-nitrophenylacetonitrile
CAS No.:22703-65-7
Molecular Formula:C₁₃H₁₆N₄O₂
Molecular Weight:260.296
Hs Code.:

α-<Bis(dimethylamino)methylene>-4-nitrophenylacetonitrile

Synonyms:α--4-nitrophenylacetonitrile

Suppliers and Price of α--4-nitrophenylacetonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α--4-nitrophenylacetonitrile

Chemical Property:

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Technology Process of α--4-nitrophenylacetonitrile

There total 4 articles about α--4-nitrophenylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 555-21-5,34512-13-5,174848-08-9
4-Nitrophenylacetonitrile

: 78581-29-0
Bis(N,N,N',N'-tetramethylformamidinium)ether-bis(trifluormethansulfonat)

: 22703-65-7
α--4-nitrophenylacetonitrile

: 632-22-4
tetramethylurea

Guidance literature:: With dimethylaminomethyl-polystyrene; In acetonitrile; at 81 ℃; for 20h;

Reference yield:

: 632-22-4
tetramethylurea

: 22703-65-7
α--4-nitrophenylacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂

2: DBU / acetonitrile; CH₂Cl₂ / 12 h / Heating

With oxalyl dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile;
DOI:10.1021/ja983016m