cis-2-phenyl-1-azidoethene

Base Information

Chemical Name:cis-2-phenyl-1-azidoethene
CAS No.:20544-50-7
Molecular Formula:C₈H₇N₃
Molecular Weight:145.164
Hs Code.:

Synonyms:cis-2-phenyl-1-azidoethene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-2-phenyl-1-azidoethene

Chemical Property:

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Technology Process of cis-2-phenyl-1-azidoethene

There total 8 articles about cis-2-phenyl-1-azidoethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 57918-63-5
(Z)-styryl iodide

: 20544-50-7
cis-2-phenyl-1-azidoethene

Guidance literature:: With copper(l) iodide; sodium azide; sodium L-prolinate; In dimethyl sulfoxide; at 70 ℃; for 2h;
DOI:10.1039/b400878b

Reference yield:

: (2-azido-2-chloroethyl)benzene

: 18756-03-1
(E)-(2-azidovinyl)benzene

: 20544-50-7
cis-2-phenyl-1-azidoethene

Guidance literature:: With potassium tert-butylate; In diethyl ether; at -20 - 0 ℃; for 2h; Overall yield = 74 %;
DOI:10.1021/acs.orglett.7b02380

Reference yield:

: 1-azido-2-phenylethanol

: 18756-03-1
(E)-(2-azidovinyl)benzene

: 20544-50-7
cis-2-phenyl-1-azidoethene

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride / chloroform / 13 h / -50 - 20 °C

2: potassium tert-butylate / diethyl ether / 2 h / -20 - 0 °C

With potassium tert-butylate; phosphorus trichloride; In diethyl ether; chloroform;
DOI:10.1021/acs.orglett.7b02380