N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

Base Information

Chemical Name:N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide
CAS No.:1208130-66-8
Molecular Formula:C₁₈H₂₆IN₇O₆
Molecular Weight:563.352
Hs Code.:

Synonyms:N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

Suppliers and Price of N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

There total 6 articles about N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.1%

: C₁₉H₂₇IN₆O₆

: 1208130-66-8
N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

Guidance literature:: With hydroxylamine potassium salt; In methanol;
DOI:10.1007/s00044-017-1999-2

Reference yield:

: 74-79-3,25212-18-4
L-arginine

: 1208130-66-8
N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid; sulfuric acid

2: acetyl chloride

3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / tetrahydrofuran / -5 °C

4: hydroxylamine potassium salt / methanol

With hydroxylamine potassium salt; sulfuric acid; nitric acid; benzotriazol-1-ol; acetyl chloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol;
DOI:10.1007/s00044-017-1999-2

Reference yield:

: 6306-52-1
L-valine methylester hydrochloride

: 1208130-66-8
N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-3-methyl-1-oxobutan-2-yl)-2-iodobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methyl-morpholine / tetrahydrofuran / -15 °C

2: sodium hydroxide; water / methanol

3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / tetrahydrofuran / -5 °C

4: hydroxylamine potassium salt / methanol

With 4-methyl-morpholine; hydroxylamine potassium salt; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1007/s00044-017-1999-2