1(2H)-Naphthalenone, 3,4-dihydro-5-methoxy-8-methyl-

Base Information

Chemical Name:1(2H)-Naphthalenone, 3,4-dihydro-5-methoxy-8-methyl-
CAS No.:53863-68-6
Molecular Formula:C12H14O2
Molecular Weight:190.242
Hs Code.:
NSC Number:135932
DSSTox Substance ID:DTXSID50300320
Wikidata:Q82043284
Mol file:53863-68-6.mol

Synonyms:53863-68-6;1(2H)-Naphthalenone, 3,4-dihydro-5-methoxy-8-methyl-;5-Methoxy-8-methyl-3,4-dihydro-1(2H)-naphthalenone;5-methoxy-8-methyl-3,4-dihydro-2H-naphthalen-1-one;5-methoxy-8-methyl-3,4-dihydronaphthalen-1(2H)-one;MFCD00820258;5-methoxy-8-methyl-1,2,3,4-tetrahydronaphthalen-1-one;NSC135932;TimTec1_005600;SCHEMBL9448294;DTXSID50300320;HADPARVFTQANAI-UHFFFAOYSA-N;HMS1549O12;5-methoxy-8-methyl-tetralin-1-one;STK728505;AKOS005524591;NSC-135932;NCGC00173063-01;NS-01773;CS-0317653;5-Methoxy-8-methyl-3,4-dihydro-1(2H)-naphthalenone #;1,2,3,4-Tetrahydronaphtalene-1-one, 5-methyloxy-8-methyl-

Suppliers and Price of 1(2H)-Naphthalenone, 3,4-dihydro-5-methoxy-8-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 10 raw suppliers

Chemical Property of 1(2H)-Naphthalenone, 3,4-dihydro-5-methoxy-8-methyl-

Chemical Property:

Vapor Pressure:7.01E-05mmHg at 25°C
Refractive Index:1.544
Boiling Point:343.5 °C at 760 mmHg
Flash Point:161.3 °C
Density:1.099 g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:190.099379685
Heavy Atom Count:14
Complexity:224

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C2C(=C(C=C1)OC)CCCC2=O

Technology Process of 1(2H)-Naphthalenone, 3,4-dihydro-5-methoxy-8-methyl-

There total 12 articles about 1(2H)-Naphthalenone, 3,4-dihydro-5-methoxy-8-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 8-methyl-5-methoxy-1-tetralol

: 53863-68-6
8-methyl-5-methoxy-1-tetralone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1080/14786419.2014.945171

Reference yield: 86.0%

: 226918-07-6
4-(2-methoxy-5-methyl-phenyl)-butyric acid tert-butyl ester

: 53863-68-6
8-methyl-5-methoxy-1-tetralone

Guidance literature:: With methanesulfonic acid; phosphorus pentoxide;
DOI:10.1021/jo9822838

Reference yield:

: 6627-55-0
2-bromo-p-cresol

: 53863-68-6
8-methyl-5-methoxy-1-tetralone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaOH / 1.) H₂O

2: 1.) t-BuLi / 1.) THF

3: 53 percent / H₂ / Pd/C / ethanol; acetic acid / 3102.89 Torr

4: 86 percent / P₂O₅, MeSO₃H

With sodium hydroxide; methanesulfonic acid; hydrogen; tert.-butyl lithium; phosphorus pentoxide; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jo9822838