Cyclohexanecarbonyl chloride, 2-(acetyloxy)-, trans- (9CI)

Base Information

Chemical Name:Cyclohexanecarbonyl chloride, 2-(acetyloxy)-, trans- (9CI)
CAS No.:114250-36-1
Molecular Formula:C9H13 Cl O3
Molecular Weight:204.65072
Hs Code.:
Mol file:114250-36-1.mol

Synonyms:Cyclohexanecarbonyl chloride, 2-(acetyloxy)-, trans- (9CI)

Suppliers and Price of Cyclohexanecarbonyl chloride, 2-(acetyloxy)-, trans- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Cyclohexanecarbonyl chloride, 2-(acetyloxy)-, trans- (9CI)

Chemical Property:

Boiling Point:253.6±33.0 °C(Predicted)
PSA：43.37000
Density:1.18±0.1 g/cm3(Predicted)
LogP:1.87370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarbonyl chloride, 2-(acetyloxy)-, trans- (9CI)

There total 1 articles about Cyclohexanecarbonyl chloride, 2-(acetyloxy)-, trans- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 114250-44-1
trans-2-(acetyloxy)-1-cyclohexanecarboxylic acid

: 114250-36-1,117241-43-7
trans-2-(acetyloxy)-1-cyclohexanecarbonyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; 1) 0 deg C, 30 min; 2) 3 h, room temperature;
DOI:10.1021/jm00402a032

Reference yield:

: 114250-36-1,117241-43-7
trans-2-(acetyloxy)-1-cyclohexanecarbonyl chloride

: 114250-40-7
trans-4a,5,6,7,8,8a-hexahydro-3-<<(phenylmethoxy)carbonyl>oxy>-4-hydroxy-2H-1-benzopyran-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine / 1) CH₂Cl₂, 30 min, room temperature; 2) CH₂Cl₂, 0 deg C, 1 h, room temperature, overnight

2: 68 percent / p-TsOH / methanol / 24 h / Heating

With pyridine; toluene-4-sulfonic acid; In methanol;
DOI:10.1021/jm00402a032

Reference yield:

: 75307-57-2
2,2-dimethyl-5-<<(phenylmethoxy)carbonyl>oxy>-1,3-dioxane-4,6-dione

: 114250-36-1,117241-43-7
trans-2-(acetyloxy)-1-cyclohexanecarbonyl chloride

: 114250-38-3
trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

Guidance literature:: With pyridine; Yield given. Multistep reaction; 1) CH₂Cl₂, 30 min, room temperature; 2) CH₂Cl₂, 0 deg C, 1 h, room temperature, overnight;
DOI:10.1021/jm00402a032