3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

Base Information

Chemical Name:3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose
CAS No.:191721-08-1
Molecular Formula:C₂₃H₂₉NO₄
Molecular Weight:383.488
Hs Code.:

Synonyms:3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

Suppliers and Price of 3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

There total 5 articles about 3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 191721-02-5
N-Benzyl-N-[(R)-1-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-ethyl]-hydroxylamine

: 191721-08-1
3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

Guidance literature:: With copper diacetate; acetic acid; zinc; In water; at 70 ℃; for 1h;
DOI:10.1016/S0957-4166(97)00147-X

Reference yield: 78.0%

: 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-O-tosyl-β-L-ido-1,4-furanose

: 100-46-9
benzylamine

: 191721-08-1
3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

Guidance literature:: at 100 ℃; for 14h;
DOI:10.1021/jo051143c

Reference yield:

: 29601-98-7
N-benzylhydroxylamine hydrochloride

: 191721-08-1
3-O-benzyl-5-benzylamino-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco-1,4-furanose

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / AcONa / ethanol; H₂O / 16 h / Ambient temperature

2: 1.) TMSOTf / 1.) THF, -10 deg C, 10 min, 2.) THF, -78 deg C

3: 80 percent / Zn, Cu(OAc)2, AcOH / H₂O / 1 h / 70 °C

With copper diacetate; trimethylsilyl trifluoromethanesulfonate; sodium acetate; acetic acid; zinc; In ethanol; water;
DOI:10.1016/S0957-4166(97)00147-X