C₆₇H₉₅IO₉

Base Information

Chemical Name:C₆₇H₉₅IO₉
CAS No.:1618096-68-6
Molecular Formula:C₆₇H₉₅IO₉
Molecular Weight:1171.39
Hs Code.:

C<sub>67</sub>H<sub>95</sub>IO<sub>9</sub>

Synonyms:C₆₇H₉₅IO₉

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Chemical Property of C₆₇H₉₅IO₉

Chemical Property:

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Technology Process of C₆₇H₉₅IO₉

There total 14 articles about C₆₇H₉₅IO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₇₂H₁₀₅IO₁₀

: 1618096-68-6
C₆₇H₉₅IO₉

Guidance literature:: C₇₂H₁₀₅IO₁₀; With hydrogenchloride; water; In tetrahydrofuran; at 50 ℃; Inert atmosphere;

With iodine; In toluene; Inert atmosphere; Reflux;
DOI:10.1021/jo501266g

Reference yield:

: 1618092-84-4
5-bromo-2-(5,5-dimethyl-1,3-dioxan-2-yl)-4-methoxyphenol

: 1618096-68-6
C₆₇H₉₅IO₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 50 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Glovebox; Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / tetrahydrofuran / 0 °C / Inert atmosphere

4.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

5.1: 2 h / 140 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

7.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

7.2: Inert atmosphere; Reflux

8.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

9.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

9.2: Inert atmosphere; Reflux

10.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

11.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

11.2: Inert atmosphere; Reflux

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; potassium tert-butylate; water; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; hexane; dimethyl sulfoxide; 1.1: |Williamson Ether Synthesis / 6.1: |Horner-Wadsworth-Emmons Olefination / 8.1: |Horner-Wadsworth-Emmons Olefination / 10.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501266g

Reference yield:

: 1618092-85-5
2-[4-bromo-2-((2-ethylhexyl)oxy)-5-methoxyphenyl]-5,5-dimethyl-1,3-dioxane

: 1618096-68-6
C₆₇H₉₅IO₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Glovebox; Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / tetrahydrofuran / 0 °C / Inert atmosphere

3.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

4.1: 2 h / 140 °C / Inert atmosphere

5.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

6.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

6.2: Inert atmosphere; Reflux

7.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

8.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

8.2: Inert atmosphere; Reflux

9.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

10.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

10.2: Inert atmosphere; Reflux

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; potassium tert-butylate; water; triphenylphosphine; In tetrahydrofuran; hexane; 5.1: |Horner-Wadsworth-Emmons Olefination / 7.1: |Horner-Wadsworth-Emmons Olefination / 9.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501266g