C₄₄H₅₀N₄O₁₁

Base Information

• Chemical Name: C₄₄H₅₀N₄O₁₁
• CAS No.: 1262657-43-1
• Molecular Formula: C₄₄H₅₀N₄O₁₁
• Molecular Weight: 810.901
• Mol file: 1262657-43-1.mol

Synonyms:C₄₄H₅₀N₄O₁₁

Chemical Property of C₄₄H₅₀N₄O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₅₀N₄O₁₁

There total 10 articles about C₄₄H₅₀N₄O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-bis(benzyloxymethyl)-4-formyl-2,3-dihydro-1H-imidazol-2-one (896141-21-2) → C44H50N4O11 (1262657-43-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

1.2: 2 h / -78 °C

2.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C

3.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere

With manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water;

DOI:10.1039/c0cc02214d

Reference yield:

C44H54N4O11 → C44H50N4O11 (1262657-43-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C

2: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere

With manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; In dichloromethane; water;

DOI:10.1039/c0cc02214d

Reference yield:

C19H20N2O3 → C44H50N4O11 (1262657-43-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: trichlorophosphate / mineral oil / 2 h / 0 - 23 °C / Inert atmosphere

1.2: 1 h / 23 °C / Cooling with ice

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

2.2: 2 h / -78 °C

3.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C

4.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere

With manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; lithium hexamethyldisilazane; trichlorophosphate; In tetrahydrofuran; dichloromethane; water; mineral oil;

DOI:10.1039/c0cc02214d

upstream raw materials:

1,3-bis(benzyloxymethyl)-4-formyl-2,3-dihydro-1H-imidazol-2-one

Benzyloxymethyl chloride

(4S)-4-formyl-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

methyl 3-[(4'R)-N-tert-butoxycarbonyl-2',2'-dimethyloxazolidin-4'-yl]propenoate

Downstream raw materials:

C₄₃H₅₃N₇O₈

C₃₆H₃₈N₈O₆

C₂HF₃O₂*C₃₆H₄₀N₆O₆

C₄₁H₄₁Br₂N₇O₇