Technology Process of C22H25N3O4
There total 8 articles about C22H25N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
isopropyl alcohol;
for 3h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: ammonia; carbon dioxide / 0.5 h / 50 °C
2.1: acetic acid; nitric acid; sulfuric acid / 10 - 45 °C
3.1: palladium 10% on activated carbon / ethanol / 0.17 h / Autoclave
3.2: 60 °C / 3750.38 - 4500.45 Torr / Autoclave
4.1: ammonium formate / 5 h / 165 °C / Inert atmosphere
5.1: trichlorophosphate / N,N-dimethyl-formamide / 110 °C
6.1: isopropyl alcohol / 3 h / Reflux
With
carbon dioxide; sulfuric acid; palladium 10% on activated carbon; ammonia; nitric acid; ammonium formate; acetic acid; trichlorophosphate;
In
ethanol; N,N-dimethyl-formamide; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid; nitric acid; sulfuric acid / 10 - 45 °C
2.1: palladium 10% on activated carbon / ethanol / 0.17 h / Autoclave
2.2: 60 °C / 3750.38 - 4500.45 Torr / Autoclave
3.1: ammonium formate / 5 h / 165 °C / Inert atmosphere
4.1: trichlorophosphate / N,N-dimethyl-formamide / 110 °C
5.1: isopropyl alcohol / 3 h / Reflux
With
sulfuric acid; palladium 10% on activated carbon; nitric acid; ammonium formate; acetic acid; trichlorophosphate;
In
ethanol; N,N-dimethyl-formamide; isopropyl alcohol;