Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester

Base Information

Chemical Name:Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester
CAS No.:552856-35-6
Molecular Formula:C₂₁H₂₆O₁₀
Molecular Weight:438.431
Hs Code.:

Synonyms:Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester

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Technology Process of Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester

There total 1 articles about Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 63593-03-3
1,2-O-isopropylidene-3-O-benzyl-4-hydroxymethyl-α-D-ribofuranose

: 552856-35-6
Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: With sulfuric acid; In acetic acid; at 20 ℃; for 2h;
DOI:10.1039/b208864a

Reference yield: 91.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 65-71-4,28806-14-6,691841-57-3
thymin

: 552856-35-6
Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester

: 552856-36-7
1-(2,5-di-O-acetyl-4-C-acetyloxymethyl-3-O-benzyl-β-D-erythro-pentofuranosyl)thymine

Guidance literature:: thymin; Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; for 1.5h; Heating / reflux;

trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 80 ℃; for 3.5h;

Reference yield: 91.0%

: 65-71-4,28806-14-6,691841-57-3
thymin

: 552856-35-6
Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester

: 552856-36-7
1-(2,5-di-O-acetyl-4-C-acetyloxymethyl-3-O-benzyl-β-D-erythro-pentofuranosyl)thymine

Guidance literature:: thymin; Acetic acid (3S,4R)-4,5-diacetoxy-2-acetoxymethyl-3-benzyloxy-tetrahydro-furan-2-ylmethyl ester; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; for 1.5h; Heating;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 80 ℃; for 3.5h; Further stages.;
DOI:10.1039/b208864a