Technology Process of 12-<2'-(Methoxymethoxy)phenyl>-1-dodecanal
There total 4 articles about 12-<2'-(Methoxymethoxy)phenyl>-1-dodecanal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
oxalyl dichloride;
In
dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 85 percent / 48 percent aqueous HBr / 12 h / 80 - 90 °C / darkness
2: 85 percent / pyridinium-p-toluenesulfonate / CH2Cl2 / 12 h / Ambient temperature
3: 85 percent / 2.5 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran
4: 1.) pyridinium p-toluenesulfonate; 2.) 80 percent MCPBA
5: oxalic acid dichloride / dimethylsulfoxide
With
n-butyllithium; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; hydrogen bromide; pyridinium p-toluenesulfonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / pyridinium-p-toluenesulfonate / CH2Cl2 / 12 h / Ambient temperature
2: 85 percent / 2.5 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran
3: 1.) pyridinium p-toluenesulfonate; 2.) 80 percent MCPBA
4: oxalic acid dichloride / dimethylsulfoxide
With
n-butyllithium; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide;
