Technology Process of C17H15BrO4S
There total 4 articles about C17H15BrO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aluminum (III) chloride; bromine / dichloromethane
2: toluene-4-sulfonic acid
3: n-butyllithium; iodine / diethyl ether
4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide
5: potassium permanganate; water; sodium hydrogencarbonate; magnesium sulfate / acetone
With
aluminum (III) chloride; bis-triphenylphosphine-palladium(II) chloride; potassium permanganate; copper(l) iodide; n-butyllithium; water; bromine; iodine; sodium hydrogencarbonate; magnesium sulfate; toluene-4-sulfonic acid; triethylamine;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone;
1: Friedel Crafts bromination;
DOI:10.1016/j.bmcl.2011.07.057
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide
2: potassium permanganate; water; sodium hydrogencarbonate; magnesium sulfate / acetone
With
bis-triphenylphosphine-palladium(II) chloride; potassium permanganate; copper(l) iodide; water; sodium hydrogencarbonate; magnesium sulfate; triethylamine;
In
N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2011.07.057
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium; iodine / diethyl ether
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide
3: potassium permanganate; water; sodium hydrogencarbonate; magnesium sulfate / acetone
With
bis-triphenylphosphine-palladium(II) chloride; potassium permanganate; copper(l) iodide; n-butyllithium; water; iodine; sodium hydrogencarbonate; magnesium sulfate; triethylamine;
In
diethyl ether; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2011.07.057