3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde

Base Information

Chemical Name:3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde
CAS No.:159425-45-3
Molecular Formula:C₂₄H₂₈O₁₀
Molecular Weight:476.48
Hs Code.:

Synonyms:3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde

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Chemical Property of 3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde

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Technology Process of 3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde

There total 11 articles about 3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 159425-44-2
3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzyl alcohol

: 159425-45-3
3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 48h;
DOI:10.1021/jo00101a032

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 159425-45-3
3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / Al₂O₃ / toluene / Heating

2: 96 percent / NaH / tetrahydrofuran; dimethylformamide

3: n-BuLi / cyclohexane; hexane / 1.) r.t., 15 min, 2.) r.t., 15 min

4: n-BuLi / tetrahydrofuran / Ambient temperature

5: 100 percent / MnO₂ / CH₂Cl₂ / 16 h / Ambient temperature

6: 93 percent / TBAF / tetrahydrofuran / 1 h / Ambient temperature

7: 84 percent / MnO₂ / CH₂Cl₂ / 48 h

With manganese(IV) oxide; n-butyllithium; tetrabutyl ammonium fluoride; sodium hydride; aluminum oxide; In tetrahydrofuran; hexane; dichloromethane; cyclohexane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo00101a032

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 159425-45-3
3,5-bis(methoxymethoxy)-4-<2-(methoxymethoxy)-6-(1,3-dioxanyl)benzoyl>benzaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / diisopropylethylamine / CH₂Cl₂ / Ambient temperature

2: 100 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

3: 87 percent / imidazole / CH₂Cl₂

4: n-BuLi / tetrahydrofuran / Ambient temperature

5: 100 percent / MnO₂ / CH₂Cl₂ / 16 h / Ambient temperature

6: 93 percent / TBAF / tetrahydrofuran / 1 h / Ambient temperature

7: 84 percent / MnO₂ / CH₂Cl₂ / 48 h

With 1H-imidazole; manganese(IV) oxide; lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00101a032