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C38H38O2

Base Information
  • Chemical Name:C38H38O2
  • CAS No.:282096-58-6
  • Molecular Formula:C38H38O2
  • Molecular Weight:526.719
  • Hs Code.:
C<sub>38</sub>H<sub>38</sub>O<sub>2</sub>

Synonyms:C38H38O2

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Chemical Property of C38H38O2
Chemical Property:
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Technology Process of C38H38O2

There total 2 articles about C38H38O2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
2-hex-1-ynyl-2-(4-vinyl-phenyl)-[1,3]dithiolane; With lithium di-n-butylcuprate; In tetrahydrofuran; at -78 ℃;
terephthalaldehyde,; In tetrahydrofuran; at -78 ℃;
With trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/ja0004736
Guidance literature:
Multi-step reaction with 2 steps
1.1: BF3*Et2O / methanol / 5 h / 20 °C
2.1: Bu2CuLi / tetrahydrofuran / 1.5 h / -78 °C
2.2: tetrahydrofuran / -78 - 20 °C
2.3: 51 percent / BF3*OEt2 / tetrahydrofuran / 20 °C
With boron trifluoride diethyl etherate; lithium di-n-butylcuprate; In tetrahydrofuran; methanol; 1.1: Substitution / 2.1: Addition / 2.2: Addition / 2.3: Cyclization;
DOI:10.1021/ja0004736
Guidance literature:
With triethylamine; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 110 ℃; for 12h;
DOI:10.1021/ja0004736
upstream raw materials:

terephthalaldehyde,

2-hex-1-ynyl-2-(4-vinyl-phenyl)-[1,3]dithiolane

Downstream raw materials:

C52H46O4

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