1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit

Base Information

• Chemical Name: 1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit
• CAS No.: 106989-07-5
• Molecular Formula: C₃₆H₄₁NO₆
• Molecular Weight: 583.725

Synonyms:1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit

Chemical Property of 1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit

Chemical Property:

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Technology Process of 1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit

There total 1 articles about 1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

Benzoic acid (1R,3S,4S,5R,6S)-3,5,6-tris-benzyloxy-3-benzyloxymethyl-2-[(E)-hydroxyimino]-4-methoxy-cyclohexyl ester (106989-06-4,107079-34-5,107079-35-6) → 1L-1-amino-2,4,5-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-3-O-methyl-myo-inosit (107079-36-7) + 1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit (106989-07-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; Yields of byproduct given; -10 deg C, 10 min then 70 deg C, 6 h;

DOI:10.1002/jlac.198719870350

Reference yield: 94.0%

1L-1-amino-3,4,6-tri-O-benzyl-6-C-(benzyloxymethyl)-1-desoxy-5-O-methyl-chiro-inosit (106989-07-5) → 1L-1-amino-1-desoxy-6-C-(hydroxymethyl)-5-O-methyl-chiro-inosit-hydrochlorid (107079-71-0)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 24h;

DOI:10.1002/jlac.198719870350

upstream raw materials:

Benzoic acid (1R,3S,4S,5R,6S)-3,5,6-tris-benzyloxy-3-benzyloxymethyl-2-[(E)-hydroxyimino]-4-methoxy-cyclohexyl ester

Downstream raw materials:

1L-1-amino-1-desoxy-6-C-(hydroxymethyl)-5-O-methyl-chiro-inosit-hydrochlorid

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