Technology Process of C19H22INO5
There total 5 articles about C19H22INO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iodine; potassium carbonate;
In
methanol; water;
at 20 ℃;
for 24h;
DOI:10.1021/ol3027945
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 °C
2.1: triethylamine / dichloromethane / 2 h / 0 °C
3.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 100 °C
4.1: potassium hydroxide / water; ethanol / 2 h / 120 °C
4.2: 4 h / 20 °C
5.1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C
6.1: iodine; potassium carbonate / methanol; water / 24 h / 20 °C
With
dimethylsulfide borane complex; iodine; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; triethylamine; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol3027945
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 100 °C
2.1: potassium hydroxide / water; ethanol / 2 h / 120 °C
2.2: 4 h / 20 °C
3.1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C
4.1: iodine; potassium carbonate / methanol; water / 24 h / 20 °C
With
dimethylsulfide borane complex; iodine; potassium carbonate; caesium carbonate; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol3027945
