4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide

Base Information

Chemical Name:4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide
CAS No.:364342-32-5
Molecular Formula:C₂₈H₂₀Br₄N₂O
Molecular Weight:720.096
Hs Code.:

Synonyms:4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide

There total 1 articles about 4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1122-91-4
4-bromo-benzaldehyde

: 364342-32-5
4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide

Guidance literature:: With ammonium acetate; In water; for 2h; Microwave irradiation; Sealed tube; Heating;
DOI:10.1016/j.bmc.2012.11.026

Reference yield: 66.0%

: 364342-32-5
4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide

: 117903-53-4
meso-1,2-bis(4-bromophenyl)-1,2-ethanediamine

Guidance literature:: 4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide; With sulfuric acid; In water; for 3h; Microwave irradiation; Sealed tube; Heating;

With sodium hydroxide; In water; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2012.11.026

Reference yield:

: 364342-32-5
4-bromo-N-(2-(4-bromobenzylideneamino)-1,2-(4-bromophenyl)ethyl)benzamide

: (4,5-bis(4-bromophenyl)-2-(2-ethoxy-4-methoxyphenyl)-4,5-dihydroimidazolyl)(4-(2-hydroxyethyl)piperazinyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / water / 3 h / Microwave irradiation; Sealed tube; Heating

1.2: 2 h / 20 °C

2.1: triethylamine; dmap / ethanol / 4 h / Microwave irradiation; Sealed tube; Heating

3.1: triethylamine / dichloromethane; toluene / 1 h / 20 °C / Inert atmosphere

3.2: 0 - 20 °C

With dmap; sulfuric acid; triethylamine; In ethanol; dichloromethane; water; toluene;
DOI:10.1016/j.bmc.2012.11.026