4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine

Base Information

• Chemical Name: 4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine
• CAS No.: 746673-81-4
• Molecular Formula: C₁₉H₁₈ClN₃O₄S
• Molecular Weight: 419.889

Synonyms:4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine

Chemical Property of 4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine

Chemical Property:

Purity/Quality:

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Technology Process of 4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine

There total 1 articles about 4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,6-dichloropyrimidine (1193-21-1) + 4-(4, 4,5, 5-tetramethyl-[1, 3,2] dioxaborolan-2-yl)-l-(2, 4, 6-trimethyl-benzenesulfonyl)-lH-pyrrole-2-carboxylic acid methyl ester (620616-04-8) → 4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine (746673-81-4)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 85 ℃; for 7h;

Reference yield:

4-chloro-6-N-mestylenesulfonamide methyl pyrrole 2'acetate pyrimidine (746673-81-4) + aniline (62-53-3) → C25H24N4O4S (1373765-05-9)

Guidance literature:

In dimethyl sulfoxide; at 75 ℃; for 6h;

upstream raw materials:

4,6-dichloropyrimidine

4-(4, 4,5, 5-tetramethyl-[1, 3,2] dioxaborolan-2-yl)-l-(2, 4, 6-trimethyl-benzenesulfonyl)-lH-pyrrole-2-carboxylic acid methyl ester

Downstream raw materials:

C₂₅H₂₄N₄O₄S

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