Technology Process of C8H13NO2
There total 2 articles about C8H13NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine
2.1: sodium periodate; ruthenium trichloride
4.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 1 h / -5 °C / Inert atmosphere
4.2: 72 h / -5 - 30 °C / Inert atmosphere
4.3: 24 h / 20 °C
5.1: water; sodium hydroxide / ethanol / 24 h
6.1: thionyl chloride
With
ruthenium trichloride; sodium periodate; thionyl chloride; water; diethylzinc; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
ethanol; hexane; dichloromethane;
3.1: Wittig reaction / 4.1: Simmons-Smith reaction / 4.2: Simmons-Smith reaction;
DOI:10.1016/j.tetlet.2012.05.020
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine
2.1: sodium periodate; ruthenium trichloride
4.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 1 h / -5 °C / Inert atmosphere
4.2: 72 h / -5 - 30 °C / Inert atmosphere
With
ruthenium trichloride; sodium periodate; diethylzinc; triethylamine; trifluoroacetic acid;
In
hexane; dichloromethane;
3.1: Wittig reaction / 4.1: Simmons-Smith reaction / 4.2: Simmons-Smith reaction;
DOI:10.1016/j.tetlet.2012.05.020
- Guidance literature:
-
With
copper(l) iodide; caesium carbonate;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 12h;
Inert atmosphere;
