C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄

Base Information

Chemical Name:C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄
CAS No.:901127-06-8
Molecular Formula:C₆₇H₉₃N₁₁O₁₅S₄
Molecular Weight:1421.79
Hs Code.:

C<sub>66</sub><sup>(13)</sup>CH<sub>93</sub>N<sub>11</sub>O<sub>15</sub>S<sub>4</sub>

Synonyms:C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄

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Chemical Property of C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄

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Technology Process of C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄

There total 4 articles about C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 901127-05-7
C₁₆⁽¹³⁾CH₁₉NO₂S₂

: Ac-Arg(Pbf)-Arg(Pbf)-Asp(Ot-Bu)-Gly-OH

: 901127-06-8
C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/ja061588y

Reference yield:

: 84771-22-2
C₁₃⁽¹³⁾CH₁₉NO₄

: 901127-06-8
C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄

Guidance literature:: Multi-step reaction with 3 steps

1: EDCI; DMAP; DIEA / dimethylformamide; CH₂Cl₂ / 20 °C

2: aq. TFA / CH₂Cl₂ / 20 °C

3: 85 percent / HATU; DIEA / dimethylformamide / 12 h / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja061588y

Reference yield:

: C₂₁⁽¹³⁾CH₂₇NO₄S₂

: 901127-06-8
C₆₆⁽¹³⁾CH₉₃N₁₁O₁₅S₄

Guidance literature:: Multi-step reaction with 2 steps

1: aq. TFA / CH₂Cl₂ / 20 °C

2: 85 percent / HATU; DIEA / dimethylformamide / 12 h / 20 °C

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja061588y