4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione

Base Information

Chemical Name:4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione
CAS No.:357277-63-5
Molecular Formula:C₂₃H₁₉NO₄
Molecular Weight:373.408
Hs Code.:

Synonyms:4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione

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Technology Process of 4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione

There total 1 articles about 4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 16511-38-9
1H-[1]benzazepin-2,5(3H,4H)-dione

: 39511-12-1
(E)-3-(furan-2-yl)-1-phenyl-2-propen-1-one

: 357277-63-5
4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione

Guidance literature:: With potassium hydroxide; In ethanol; at 20 ℃; for 7h;
DOI:10.1002/1521-4184(200105)334:5<163::AID-ARDP163>3.0.CO;2-3

Reference yield: 72.0%

: 357277-63-5
4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione

: 357277-64-6
4-furan-2-yl-2-phenyl-5,7-dihydro-1,7-diaza-dibenzo[a,c]cyclohepten-6-one

Guidance literature:: With ammonium ferric sulfate; ammonium acetate; In acetic acid; for 3h; Heating;
DOI:10.1002/1521-4184(200105)334:5<163::AID-ARDP163>3.0.CO;2-3

Reference yield:

: 357277-63-5
4-[1-(2-furyl)-3-oxo-3-phenyl-propyl]-1H-[1]benzazepine-2,5(3H,4H)-dione

: 2-phenyl-5,7-dihydro-1,7-diaza-dibenzo[a,c]cyclohepten-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / NH₄Fe(SO₄)2*12H₂O; NH₄OAc / acetic acid / 3 h / Heating

2: 40 percent / KMnO₄ / 2-methyl-propan-2-ol; H₂O / 2 h / 75 - 80 °C

3: 34 percent / copper chromite / quinoline / 6 h / Heating

With potassium permanganate; ammonium ferric sulfate; ammonium acetate; copper chromite; In quinoline; water; acetic acid; tert-butyl alcohol;
DOI:10.1002/1521-4184(200105)334:5<163::AID-ARDP163>3.0.CO;2-3