5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine

Base Information

Chemical Name:5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine
CAS No.:872042-75-6
Molecular Formula:C₂₉H₄₂N₂O₈SeSi₃
Molecular Weight:709.878
Hs Code.:

Synonyms:5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine

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Chemical Property of 5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine

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Technology Process of 5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine

There total 2 articles about 5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 393802-86-3
2'-deoxy-2'-methylselanyluridine

: 309963-45-9
benzhydryloxy-bis(trimethylsilyloxy)silyl chloride

: 872042-75-6
5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ol052270y

Reference yield:

: 393802-82-9
5'-O-(4,4'-dimethoxytrityl)-2'-deoxy-2'-Se-methoxyuridine

: 872042-75-6
5'-O-bis(trimethylsiloxy)benzhydroxysilyl-2'-deoxy-2'-methylselanyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / aq. AcOH / 2 h / 20 °C

2: 86 percent / pyridine / dimethylformamide / 20 °C

With pyridine; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/ol052270y