potassium 4-(1-nonyl)phenyltrifluoroborate

Base Information

• Chemical Name: potassium 4-(1-nonyl)phenyltrifluoroborate
• CAS No.: 1173195-26-0
• Molecular Formula: C₁₅H₂₃BF₃*K
• Molecular Weight: 310.252
• Mol file: 1173195-26-0.mol

Synonyms:potassium 4-(1-nonyl)phenyltrifluoroborate

Chemical Property of potassium 4-(1-nonyl)phenyltrifluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of potassium 4-(1-nonyl)phenyltrifluoroborate

There total 1 articles about potassium 4-(1-nonyl)phenyltrifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

4-bromo-1-(1-nonyl)benzene (51554-94-0) → potassium 4-(1-nonyl)phenyltrifluoroborate (1173195-26-0)

Guidance literature:

4-bromo-1-(1-nonyl)benzene; With n-butyllithium; In diethyl ether; hexane; at 20 ℃; Inert atmosphere; Cooling;

With Triisopropyl borate; In tetrahydrofuran; diethyl ether; hexane; at 20 ℃; for 1.5h; Inert atmosphere; Cooling;

With potassium hydrogen bifluoride; In tetrahydrofuran; diethyl ether; hexane; water; Inert atmosphere;

DOI:10.1002/chem.200900022

Reference yield: 44.0%

potassium 4-(1-nonyl)phenyltrifluoroborate (1173195-26-0) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → 1-(4-n-nonylphenyl)-1,9-dihydro[60]fullerene (1171848-68-2)

Guidance literature:

With bis(acetonitrile)(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In water; 1,2-dichloro-benzene; at 60 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.200900022

upstream raw materials:

4-bromo-1-(1-nonyl)benzene

Downstream raw materials:

1-(4-n-nonylphenyl)-1,9-dihydro[60]fullerene