C₃₄H₃₇NO₅Si

Base Information

Chemical Name:C₃₄H₃₇NO₅Si
CAS No.:144127-38-8
Molecular Formula:C₃₄H₃₇NO₅Si
Molecular Weight:567.757
Hs Code.:

C<sub>34</sub>H<sub>37</sub>NO<sub>5</sub>Si

Synonyms:C₃₄H₃₇NO₅Si

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Chemical Property of C₃₄H₃₇NO₅Si

Chemical Property:

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Technology Process of C₃₄H₃₇NO₅Si

There total 4 articles about C₃₄H₃₇NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130031-63-9
C₂₆H₁₉NO₄

: 144127-38-8
C₃₄H₃₇NO₅Si

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / cesium carbonate, 18-crown-6 / acetonitrile / 10 h / Ambient temperature

2: 0.5 N aq. LiOH / tetrahydrofuran / 0.5 h / 0 °C

3: triphenylphosphine / CH₂Cl₂ / 0.5 h / 0 °C

4: 68 percent / sodium borohydride / CH₂Cl₂; propan-2-ol / 0.5 h / 0 °C

5: 99 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / -78 - 0 °C

With 2,6-dimethylpyridine; lithium hydroxide; sodium tetrahydroborate; 18-crown-6 ether; caesium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; isopropyl alcohol; acetonitrile;
DOI:10.1021/ja00049a022

Reference yield:

: 132938-55-7
C₃₃H₂₄N₂O₅S

: 144127-38-8
C₃₄H₃₇NO₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / sodium borohydride / CH₂Cl₂; propan-2-ol / 0.5 h / 0 °C

2: 99 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / -78 - 0 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; In dichloromethane; isopropyl alcohol;
DOI:10.1021/ja00049a022

Reference yield:

: 141328-76-9
C₂₈H₂₁NO₆

: 144127-38-8
C₃₄H₃₇NO₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine / CH₂Cl₂ / 0.5 h / 0 °C

2: 68 percent / sodium borohydride / CH₂Cl₂; propan-2-ol / 0.5 h / 0 °C

3: 99 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / -78 - 0 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; triphenylphosphine; In dichloromethane; isopropyl alcohol;
DOI:10.1021/ja00049a022