N'-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulfonohydrazide

Base Information

• Chemical Name: N'-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulfonohydrazide
• CAS No.: 957066-12-5
• Molecular Formula: C₁₇H₂₆N₂O₂S
• Molecular Weight: 322.472
• Hs Code.: 2935009090
• Mol file: 957066-12-5.mol

Synonyms:N’-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulfonohydrazide;N’-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulphonohydrazide

Chemical Property of N'-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulfonohydrazide

Chemical Property:

• Vapor Pressure: 2.73E-08mmHg at 25°C
• Melting Point: 135-137掳C
• Refractive Index: 1.565
• Boiling Point: 450°Cat760mmHg
• Flash Point: 226°C
• PSA: 66.91000
• Density: 1.15g/cm³
• LogP: 5.31800
• Storage Temp.: Keep Cold

Purity/Quality:

97% ^*data from raw suppliers

N'-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulfonohydrazide 95+% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N'-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulfonohydrazide

There total 3 articles about N'-(4,4-Dimethylcyclohexylidene)-2,4,6-trimethylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-trimethylbenzenesulfonohydrazide (16182-15-3) + 4,4-dimethylcyclohexane-1-one (4255-62-3) → C17H26N2O2S (957066-12-5)

Guidance literature:

With sulfuric acid; In 2-methoxy-ethanol; acetonitrile; at 25 ℃; stereoselective reaction;

DOI:10.15227/orgsyn.074.0217

Reference yield:

2-mesitylenesulphonyl chloride (773-64-8) → C17H26N2O2S (957066-12-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran / 0.75 h / -10 - 25 °C

2: sulfuric acid / acetonitrile; 2-methoxy-ethanol / 25 °C

With sulfuric acid; hydrazine hydrate; In tetrahydrofuran; 2-methoxy-ethanol; acetonitrile;

DOI:10.15227/orgsyn.074.0217

Reference yield:

1,3,5-trimethyl-benzene (108-67-8) → C17H26N2O2S (957066-12-5)

Guidance literature:

Multi-step reaction with 3 steps

1: chlorosulfonic acid / -10 - 60 °C

2: hydrazine hydrate / tetrahydrofuran / 0.75 h / -10 - 25 °C

3: sulfuric acid / acetonitrile; 2-methoxy-ethanol / 25 °C

With chlorosulfonic acid; sulfuric acid; hydrazine hydrate; In tetrahydrofuran; 2-methoxy-ethanol; acetonitrile;

DOI:10.15227/orgsyn.074.0217

upstream raw materials:

2,4,6-trimethylbenzenesulfonohydrazide

4,4-dimethylcyclohexane-1-one

2-mesitylenesulphonyl chloride

1,3,5-trimethyl-benzene

Downstream raw materials:

4,4-dimethylcyclohexane-1-carbonitrile